Pop-Up Detector Test Report

Version 2.0 -- 25 June 2000
C. Darren Dowell
Caltech, Mail Code 320-47
Pasadena, CA 91125
(626)395-6675 (office)
(626)395-2600 (lab)
(626)796-8806 (FAX)
cdd@submm.caltech.edu

Abstract

Measurements of semiconducting pop-up bolometers were performed at Caltech in April 2000. We report the resistance vs. temperature and the thermal characteristics of the measured samples. The desired SHARCII and HAWC parameters were bracketed with the measured samples, and we make recommendations for the bolometer designs for the two instruments.

Acknowledgments

Walter Collins (Caltech), Mino Freund (Goddard), Matt Gardner (Caltech), and Jeff Groseth (Caltech) helped considerably with preparing the test components and in performing the measurements. Attila Kovacs (Caltech) wrote the software to solve for bolometer parameters from measured data. Christine Allen (Goddard) provided the bolometer samples and advice for handling them. Harvey Moseley (Goddard) provided guidance through the testing period. This research was funded in part by NSF grant AST 9615025 to the Caltech Submillimeter Observatory.

Outline

  1. Measurement apparatus
  2. Bolometer design
  3. Thermistor screening results
  4. Results for 5327 G0 test array
  5. Results for 5347 G0 test array
    1. Fitted parameters
    2. White noise
    3. Time constants
  6. Results for 5347 thermistor test array
  7. Measurements of absorbers
    1. Results for 5347 thermistor test array
  8. General conclusions
  9. Recommendation for SHARCII bolometer design
  10. Recommendation for HAWC bolometer design
  11. References

Measurement Apparatus

Implant and bolometer samples were tested in the SHARCII cryostat, which contains a 3He refrigerator enclosed in a L4He-cooled radiation shield. For most measurements, the main L4He reservoir was pumped down to 1.5 K so that the device substrate reached temperatures as low as 0.325 K.

implant test devices bolometer test devices package with cover on
Figure 1. Caltech interface substrate (alumina). The 3-element implant screening devices were GE varnished to the substrate, and the 32-element bolometer arrays were clipped to the substrate. Gold wedge bonds provided electrical connection between the devices, load resistors, and substrate. Surface-mount connectors were initially used to interface with the cryostat wiring. However, they were replaced with directly soldered wires for later measurements. The ceramic substrate was enclosed in an INVAR box. A sheet of gold leaf and the force of ~6 screws were used to thermally connect the INVAR and ceramic.

assembly, shield off assembly, shield on
Figure 2. Device suspension and shielding. The ceramic/ INVAR package was suspended from the L4He coldplate with 3-4 fiberglass tubes with A/L = 0.014-0.018 cm. The package was heat sunk to the fridge through an annealed OFHC copper strap with A/L = 0.014 cm. A calibrated LakeShore GRT was attached to the ceramic substrate with a screw and gold leaf, approximately 5 cm from the detectors. The package was shielded by a secondary L4He enclosure with blackened walls. With this configuration, the coldest observed GRT measurement for the detector package was 0.325 K, during which the L4He bath was at 1.5 K, the fridge was at 0.291 K, and the extrapolated parasitic heat load on the detector package was 2-4 microW. The JFET modules were located outside the inner shield.

device on coldhead
Figure 3. Additional implant screening hardware. In order to confirm the implant resistances, the 3-element devices in the Goddard-selected ceramic package were clipped to a copper block and installed directly on the SHARC II fridge coldhead or in a separate L4He cryostat (the purple 'Barney' Dewar).

All wires going into the Dewar pass through one or two RFI-filtered connectors, which contain 4 nF capacitors from each pin to the Dewar wall.

Thermal Performance of Detector Package

The silicon frame has a thickness of 300 microns. In the direction of heat flow from bolometer 1 to bolometer 32, the relevant A/L is 0.0035 cm. For a 0.3 K thermal conductivity of XXX...

The wirebonds were 0.001 inch diameter 99.99% gold. With 64 each 3 mm long wire bonds (total A/L=0.001 cm), and assuming a 0.3 K thermal conductivity of 0.1 W/cm/K (Touloukian et al. 1970), the effective G of the wirebonds was 100 microW/K. We have ignored unknown boundary thermal resistance, which will reduce the effective G.

The ceramic substrate is approximately 7 cm x 7 cm x 0.06 cm, giving an A/L of 800 cm in the thickness (shortest) direction. Assuming a 0.3 K thermal conductivity of 11 microW/cm/K (Locatelli et al. 1976), the thermal conductance from the INVAR enclosure to the trace side of the ceramic board is G = 9000 microW/K. Again, we have ignored boundary thermal resistance.

The heat strap also limits the cooling of the detector wafer. During the cooldowns reported here, the fridge/heat strap combination was observed to have an effective G of 80 microW/K at the coldest temperatures.

Combining the effective G's of the wire bonds, ceramic board, and heat strap, we estimate an effective G of 40 microW/K for the link from the silicon die to the 3He fridge, three orders of magnitude greater than the G of the membrane devices. For a maximum 0.5 V bias across the 64 each 30 Mohm load resistors and detectors, the dissipated power can be at most 0.5 microW, leading to a temperature rise of at most 13 mK. For the 0.5 V bias, the detector package was observed to slowly warm a few mK. However, the measurements with the 0.5 V bias were performed quickly, using the thermal inertia of the detector package to keep the detector cool.


Designs of Test Bolometers

Three types of bolometer arrays were manufactured for the detector measurements: The metallization of the measured wafers was aluminum.

G0 recipes
Table 1. Recipes for bolometers on G0 test arrays.

thermistor recipes
Table 2. Recipes for bolometers on thermistor test arrays.

thermistor recipes
Table 3. Implant doses. Higher net density means greater implant dose, which means lower cold resistance. Wafers 5347 and 5327 are of interest for SHARCII and HAWC. (Wafer 5168 was not tested.)


Thermistor Screening Results

The first part of the detector measurement program was to screen five wafers for desired resistance at cold temperatures. Three-element membrane devices were measured in three configurations -- GE varnished to the Caltech ceramic interface board, packaged in the Goddard ceramic carrier on a copper block in the purple L4He Dewar, and in the Goddard carrier/copper block on the SHARCII coldhead.

Resistance measurements were made with a Keithley 616 Digital Electrometer borrowed from Goddard that allows current excitations from 1 pA to 1 microA stepped by factors of 10. The reported measurements were made with the highest current setting which did not cause significant self heating. The criterion was to allow no more than a 2% effect on the observed resistance.

SHARCII Dewar, Large Ceramic Board

SHARCII Dewar implant tests
Figure 4. Resistance measurements for 3-element membrane devices on Caltech ceramic board. The SHARCII target curve is T0 = 40 K, R0 = 1430 ohm (Moseley et al. 1999), and the HAWC target is T0 = 30 K, R0 = 700 ohm (Moseley 1999).

SHARCII Dewar implant tests 2
Figure 5. Resistance measurements plotted in units which give linear fits.

A fit to the data with model R = R0 exp[(T0/T)1/2] yields:

Label   ND   R0 (ohms)  T0 (K)
-----  ----  ---------  ------
5250a  0.6     2570      81.8
5250b  0.6     3880      74.6
5327   0.7     1750      48.9
5347   0.75    2090      25.7
Table 4. Fits for resistance of implant devices on Caltech ceramic board.

Purple Dewar, Small Ceramic Package

Three-element dies were tested using the Goddard-provided ceramic packages attached 'upside down' to a copper block in order to shield the devices from radiation. Resistances were measured with the Keithley 616 electrometer.

purple Dewar implant tests 2
Figure 6. Measurements of thermistor samples in the purple Dewar.

A fit to the data from the purple Dewar experiment only yields:

Label   ND   R0 (ohms)  T0 (K)
-----  ----  ---------  ------
5306   0.65    1670      67.3
5327   0.7     2100      42.7
5347   0.75    2380      23.2
Table 5. Purple Dewar thermistor fits.

SHARCII Dewar, Small Ceramic Package on Coldhead

SHARCII coldhead implant tests
Figure 7. Measurements of thermistor sample on the SHARC II coldhead. The coldest measured temperature was 0.291 K.

Label   ND   R0 (ohms)  T0 (K)
-----  ----  ---------  ------
5347   0.75    2430      22.5
Table 6. SHARCII coldhead thermistor fit.

Comparison of Samples

Comparison of 5327 implant tests
Figure 8. Measurements of 5327 thermistor samples. Two membrane dies and one 32-element bolometer array were measured. The fits for the bolometer array represent the extreme values for the array. There is reasonable agreement among the different samples. The resistance is too high for both HAWC and SHARCII.

Comparison of 5347 implant tests
Figure 9. Measurements of 5347 thermistor samples. Two membrane dies and three 32-element arrays were measured. (The thermistor array measurements were normalized to L/W = 1.45.) There is considerable variation from sample to sample, which nearly covers the range from the HAWC target to the SHARC II target. There is good agreement between the measurements for membrane die A in the purple Dewar (green curve) and SHARC II (black curve).


Results for 5327 G0 Test Array LH5

For tests of G0 array 5327 LH5 (ND=0.7), the silicon frame was clipped to the detector board with beryllium-copper clips and gold wedge bonded. Bolometers 17-29 and 32 were wired in series with 150 Mohm SiCr load resistors from MSI. The resistance of a SiCr load varies with temperature (up to 210 Mohms at 0.33 K); this effect was measured for a few resistors and modeled for all of them in the analysis.

IV measurement circuit
Figure 10. Circuit used to measure IV curves. 16 JFETs were available, so up to 16 bolometers were measured simultaneously. The JFET gain was approximately 0.996. The bias voltage was slowly stepped from 0 V to a nonzero value. The change in voltage from the JFET gives the bolometer voltage, which yields the bolometer resistance since the load resistance is known (to 5% accuracy).

IV's for 5327 LH5
Figure 11. Sample IV curves for all bolometers at a single temperature.

IV's for 5327 LH5 bolometer 24
Figure 12. IV curves for a bolometer at multiple temperatures. The filled circles are measured data, and the lines are model fits with 4 free parameters.

The bolometer parameters are derived from a minimization procedure in which the measured I's and V's are compared with a best-fit four-parameter model. The model is:

See Mather (1982) for further details of the model.
G0 test array 5327 LH5
Data at 328, 342, 389, 467, 651, 860, 962, 4127 mK
Negative data included; 4127 mK duplicated
Updated 1 May 2000, 16:30 PDT

R = R0 exp(sqrt(T0/T))
G = G0 T^beta

                        R*     R
          R0    T0    0.3 K  0.5 K   G0=G(1 K)          G(0.3 K)*  G(0.5 K)
bol/grp  ohms    K    Mohms  Mohms  W/K^(beta+1)  beta     W/K       W/K
-------  ----  -----  -----  -----  ------------  ----  ---------  ---------
17 HG2D  1195  51.45   582    30.4    62.3 e-9    2.85   2.02 e-9   8.64 e-9
18 HG2D  1222  51.62   608    31.6    61.9 e-9    2.84   2.03 e-9   8.65 e-9
19 HG2D  1289  50.52   557    29.9    59.0 e-9    2.70   2.29 e-9   9.08 e-9
20 HG2C  1481  48.99   525    29.5     1.56e-9    1.18   0.38 e-9   0.69 e-9
21 HG2C  1321  50.76   589    31.4     1.66e-9    1.31   0.34 e-9   0.67 e-9
22 HG2C  1316  50.67   580    31.0     1.68e-9    1.31   0.35 e-9   0.68 e-9
23 HG2B  1412  49.70   549    30.2     1.61e-9    1.25   0.36 e-9   0.68 e-9
24 HG2B  1474  49.36   549    30.4     1.57e-9    1.23   0.36 e-9   0.67 e-9
25 HG2B  1363  50.43   582    31.3     1.62e-9    1.30   0.34 e-9   0.66 e-9
26 HG2A  1277  51.60   634    33.0    59.9 e-9    2.81   2.03 e-9   8.54 e-9
27 HG2A  1358  51.20   640    33.7    57.5 e-9    2.74   2.12 e-9   8.61 e-9
28 HG2A  1336  50.88   605    32.1    58.8 e-9    2.71   2.25 e-9   8.99 e-9
29 HG1A  1290  51.96   670    34.5    24.2 e-9    2.63   1.02 e-9   3.91 e-9
32  mem. 1299  51.76   658    34.1   202   e-9    2.31  12.5  e-9  40.7  e-9

* extrapolation
Table 7. Four-parameter fits for G0 bolometer array 5327 LH5.

The fits in Table 7 are somewhat unsatisfactory, as evidenced by the systematic underestimate of the bolometer resistance at the lowest and highest temperatures (Figure 12). Better fits are obtained with a slightly different thermistor behavior, such as R = R0 exp[(T0/T)0.59]. Alternatively, we fit just the data at the colder temperatures to achieve better accuracy there.

IV's for 5327 LH5 bolometer 24
Figure 13. IV curves for bolometer 24, with fit to low temperature data only (T < 0.8 K).

G0 test array 5327 LH5
Data at 328, 342, 389, 467, 651 mK
Updated 1 May 2000, 16:40 PDT

R = R0 exp(sqrt(T0/T))
G = G0 T^beta
                        R*     R
          R0    T0    0.3 K  0.5 K   G0=G(1 K)          G(0.3 K)*  G(0.5 K)
bol/grp  ohms    K    Mohms  Mohms  W/K^(beta+1)  beta     W/K       W/K
-------  ----  -----  -----  -----  ------------  ----  ---------  ---------
17 HG2D   599  58.28   677    29.3   123   e-9    3.63   1.56 e-9   9.93 e-9
18 HG2D   539  59.68   720    29.9   135   e-9    3.72   1.53 e-9  10.2  e-9
19 HG2D   590  58.26   665    28.8   129   e-9    3.61   1.67 e-9  10.6  e-9
20 HG2C   581  58.39   665    28.7     2.44e-9    1.72   0.31 e-9   0.74 e-9
21 HG2C   580  59.08   721    30.5     2.46e-9    1.78   0.29 e-9   0.72 e-9
22 HG2C   589  58.76   705    30.1     2.47e-9    1.76   0.30 e-9   0.73 e-9
23 HG2B   587  58.51   682    29.3     2.45e-9    1.76   0.29 e-9   0.72 e-9
24 HG2B   597  58.46   689    29.6     2.41e-9    1.75   0.29 e-9   0.72 e-9
25 HG2B   596  58.78   715    30.5     2.40e-9    1.77   0.28 e-9   0.70 e-9
26 HG2A   632  58.62   744    31.9   118   e-9    3.60   1.55 e-9   9.73 e-9
27 HG2A   636  58.80   765    32.6   120   e-9    3.60   1.57 e-9   9.90 e-9
28 HG2A   627  58.44   722    31.1   124   e-9    3.58   1.67 e-9  10.4  e-9
29 HG1A   630  59.22   796    33.6    42.6 e-9    3.30   0.80 e-9   4.33 e-9
32 mem.   650  58.62   765    32.8   610   e-9    3.54   8.60 e-9  52.4  e-9

* extrapolation
Table 8. Four-parameter fits for array 5327 LH5, using only data at T < 0.8 K.

The fits using only the low temperature data give 0.3 K resistances which are ~20% higher, 0.5 K resistances which are ~2% lower, 0.3 K G's which are ~25% lower, and 0.5 K G's which are ~15% higher.

The derived values of beta are somewhat surprising. The devices with only silicon legs have measured beta's of 1.3 - 1.8, while beta's of 3 (the value expected for a dielectric) were measured in the 12 micron silicon bolometers (e.g., Wang et al. 1996). The speculation is that the thermal conductance is dominated by the heavily doped traces, which have a metallic beta of 1 (H. Moseley, private communication).

The devices with metal on the legs, on the other hand, have steep beta's of 2.7 - 3.6. While normal metals should give a beta of 1, the aluminum metallization is superconducting at these temperatures and may have a much more steep beta.

The addition of 100 micron wide metal to the strap has essentially no effect on the thermal conductance. A bolometer with the design HGUNIT.2D (metal) has the same G as HGUNIT.2A (no metal), and HGUNIT.2C (metal) has the same G as HGUNIT.2B (no metal).


Parameter Fits for 5347 G0 Test Array LH1

All bolometers were wired with 30 Mohm nichrome load resistors from MSI. The nicrohme resistors are much more temperature stable, and their resistance is known to 1% accuracy. The full array was measured with two separate cooldowns between which the routing of the 16 JFETs was changed.

IV's for 5347 LH1
Figure 14. Sample IV curves for all bolometers at a single temperature.

IV's for 5347 LH1 bolometer 23
Figure 15. Sample IV curves for a single bolometer at multiple temperatures.

G0 test array 5347 LH1
Data at 330, 440, 597, 742, 985, 4243 mK (pixels 1-16)
Data at 329, 448, 604, 744, 974, 4261 mK (pixels 17-32)
Updated 1 May 2000, 16:50 PDT

R = R0 exp(sqrt(T0/T))
G = G0 T^beta

                        R*     R
          R0    T0    0.3 K  0.5 K   G0=G(1 K)          G(0.3 K)*  G(0.5 K)
bol/grp  ohms    K    Mohms  Mohms  W/K^(beta+1)  beta     W/K       W/K
-------  ----  -----  -----  -----  ------------  ----  ---------  ---------
01 mem.  1844  26.25   21.3   2.59    23.3 e-9    0.55  12.1  e-9  15.9  e-9
02 TH.1  1290  25.58   13.2   1.65     1.07e-9    1.32   0.22 e-9   0.43 e-9
03 TH.1  1365  25.51   13.8   1.73     1.20e-9    1.19   0.29 e-9   0.53 e-9
04 TH.1  1401  25.31   13.7   1.72     0.94e-9    1.15   0.24 e-9   0.42 e-9
05 HG3D  1953  26.94   25.5   3.01    24.4 e-9    1.97   2.28 e-9   6.23 e-9
06 HG3D  1956  27.16   26.5   3.11    24.1 e-9    1.96   2.28 e-9   6.19 e-9
07 HG3D  2147  27.11   28.9   3.39    19.4 e-9    1.77   2.30 e-9   5.69 e-9
08 HG3C  2127  26.93   27.7   3.27     2.24e-9    1.20   0.53 e-9   0.98 e-9
09 HG3C  1844  27.58   26.9   3.10     2.66e-9    1.38   0.51 e-9   1.02 e-9
10 HG3C  1898  27.05   25.2   2.97     2.61e-9    1.35   0.51 e-9   1.02 e-9
11 HG3B  1934  28.40   32.5   3.63    24.2 e-9    2.03   2.10 e-9   5.93 e-9
12 HG3B  1908  28.51   32.7   3.63    25.1 e-9    2.06   2.10 e-9   6.02 e-9
13 HG3B  1869  28.76   33.4   3.68    27.8 e-9    2.14   2.11 e-9   6.31 e-9
14 HG3A  1840  28.67   32.4   3.58     4.08e-9    1.44   0.72 e-9   1.50 e-9
15 HG3A  1951  28.41   32.9   3.66     3.80e-9    1.42   0.69 e-9   1.42 e-9
16 HG3A  1924  28.37   32.2   3.59     3.89e-9    1.41   0.71 e-9   1.46 e-9
17 HG2D  1893  28.73   33.7   3.71    38.4 e-9    2.63   1.62 e-9   6.20 e-9
18 HG2D  1899  28.90   34.8   3.80    38.7 e-9    2.66   1.57 e-9   6.12 e-9
19 HG2D  1981  28.82   35.8   3.93    36.7 e-9    2.65   1.51 e-9   5.85 e-9
20 HG2C  2025  28.51   34.7   3.85     1.17e-9    1.35   0.23 e-9   0.46 e-9
21 HG2C  1839  28.97   34.1   3.72     1.31e-9    1.43   0.23 e-9   0.49 e-9
22 HG2C  1920  28.91   35.2   3.85     1.26e-9    1.40   0.23 e-9   0.48 e-9
23 HG2B  1957  29.47   39.4   4.22     1.21e-9    1.37   0.23 e-9   0.47 e-9
24 HG2B  2038  29.15   38.9   4.22     1.17e-9    1.34   0.23 e-9   0.46 e-9
25 HG2B  1929  29.84   41.4   4.37     1.25e-9    1.40   0.23 e-9   0.47 e-9
26 HG2A  1871  30.40   44.0   4.55    42.4 e-9    2.76   1.53 e-9   6.26 e-9
27 HG2A  2019  29.93   44.0   4.63    37.3 e-9    2.62   1.59 e-9   6.07 e-9
28 HG2A  1952  30.41   46.0   4.76    40.0 e-9    2.69   1.57 e-9   6.20 e-9
29 HG1A  1836  31.16   49.0   4.92    20.0 e-9    2.74   0.74 e-9   2.99 e-9
30 HG1A  1788  31.95   54.2   5.30    20.7 e-9    2.80   0.71 e-9   2.97 e-9
31 HG1A  1927  31.34   52.9   5.29    18.1 e-9    2.68   0.72 e-9   2.82 e-9
32 mem.  1814  32.12   56.5   5.49    72.9 e-9    1.58  10.9  e-9  24.4  e-9

* extrapolation
Table 9. Four-parameter fits for G0 bolometer array 5347 LH1.

Although the measured values of G make qualitative sense, the scaling with leg geometry is not what was expected. This will be discussed further in the Conclusions.

Resistance Gradient

The cold resistance goes from high at bolometer 32 to low at bolometer 1. In order to confirm this situation, a few bolometers were measured individually with an electrometer. The 0.327 K resistance measured in the linear portion of the IV curve is tabluated below:
           Electrometer  Table 9 Fit
            Resistance   Resistance
Bolometer      Mohm         Mohm
---------  ------------  -----------
    1          15.6         14.4
    9          19           18.0
   12          23           21.7
   15          22           21.8
   24          28           25.7
   32          36.4         36.6
Table 10. Resistance gradient in G0 array 5347 LH1.

A radiation gradient as the cause of the resistance can be ruled out since the membrane (high G) devices and bolometers (low G) are affected about the same. WHAT ABOUT A TEMPERATURE GRADIENT???


Noise for 5347 G0 Test Array LH1

Differential DC-biased readout
Figure 16. Differential readout used for noise measurements. The differential readout was the only one available with the desired bandwidth (lowpass filtering at ~250 Hz), but it has the advantage of common mode noise rejection of bias fluctuations and microphonics.

Noise for 5347 HGUNIT2C
Figure 17. Noise spectra for bolometers 22-21 on 5347 G0 array LH1. The bolometers are of type HGUNIT2C. The observed noise has been divided by the amplifier gain (except the low pass filtering) and by 21/2 to show the noise for a single bolometer referred to the JFET input. The 1/f noise in the 40 mV and 157 mV spectra is most likely due to operation of the JFETs at a non-optimal temperature. The short horizontal lines at right show the noise predicted from the IV curve fits in the ~30 Hz region. The predictions are in good agreement with the observations. The calculated electrical NEP for the optimal 40 mV bias is 6.1x10-17 W s1/2.


Time Constants for 5347 G0 Test Array LH1

Time constant measurement circuit
Figure 18. Circuit used for time constant measurements.

For the time constant measurements, the bolometers were driven using a bias waveform with a square profile switching between two positive levels 8 mV apart. The output of the JFET was sent to an SR560 preamplifier with a gain of 100 and then to an oscilloscope. DC coupling was used on both instruments; a DC level from a power supply was subtracted to bring the signal on scale. Low-pass filtering was applied with the SR560, but the cutoff frequency (typically 3 kHz) was chosen so that only high frequency noise was eliminated and the shape of the waveform was preserved.

Additional filtering of the bolometer waveform was caused by the bias waveform filtering (cutoff frequency at 6800 Hz) and the RFI connectors (cutoff frequency at 20 kHz, assuming a 1000 ohm JFET output impedance). These cutoff frequencies are high enough to be irrelevant.

tau: bol. 24, 40 mV
Figure 19. Typical oscilloscope trace during time constant measurement. Shown is the output of the JFET for bolometer 24 of the 5347 G0 test array, multiplied by a gain of 100. The bias frequency was 8 Hz, and the settling time was 3.6 msec.

The overshoot is caused by the high-frequency impedance of the bolometer being larger than the low-frequency impedance (Mather 1982). Stated another way, the dynamic circuit model of a bolometer contains an effective inductance, which creates a voltage spike at the transition of the bias. Our interpretation is that the settling time of the voltage following the bias transition is the true detector time constant (taue in the notation of Mather 1982).

For the measured quantities, we looked at the transition caused by the positive change in the bias. We recorded:

In the table below, voltages are referred to JFET output, before the preamplification. The calculated G and T are the estimates from the IV curve fits.
                                                     calc.   observ.
            bias  calc G  calc T  V(o.s.)  t(o.s.)  V(step)  V(step)  t(settle)
bol.  grp.   mV    nw/K      K       mV      msec      mV       mV       msec
----  ----  ----  ------  ------  -------  -------  -------  -------  ---------
  9    3C    25     0.59   0.34     0.12     2.2      2.9      2.7       1.5
  9    3C    49*    0.64   0.36     0.42     1.1      1.4      1.4       1.6
  9    3C    98     0.76   0.40     0.70     0.52     0.34     0.40      1.2
  9    3C   196     0.98   0.48     0.61     0.28     0.02     0.06      0.71

 15    3A    39     0.84   0.34     0.19     1.8      2.2      2.2       1.6
 15    3A    78?*   0.95   0.38     2.8?     0.92     0.90     6.6?      1.1 
 15    3A   157     1.20   0.44     0.69     0.31     0.12     0.18      0.61
 15    3A   314     1.60   0.54     0.47     0.24    -0.02     0.05      0.31

 18    2D    49     2.1    0.34     N.A.     N.A.     2.7      2.6       0.38
 18    2D    98*    2.5    0.36     0.20     0.8      1.5      1.5       0.68
 18    2D   196     3.6    0.41     0.46     0.31     0.45     0.53      0.36
 18    2D   392     5.6    0.48     0.34     0.22     0.12     0.22      0.16

 24    2B    20     0.28   0.34     0.39     2.4      2.6      2.7       4.5
 24    2B    39*    0.31   0.37     1.1      1.3      1.2      1.1       3.6
 24    2B    78     0.38   0.43     1.2      0.6      0.17     0.11      2.3
 24    2B   157     0.50   0.53     0.74     0.4     -0.03    -0.13      1.3

* optimum bias for NEP
? apparent errors in measurement, probably bias amplitude setting
Table 11. Time constant measurements for G0 array 5347 LH1 operated at 0.328 K.

Results for 5347 Thermistor Test Array RH7

Fitted Parameters

Thermistor test array 5347 RH7
Data at 330, 451, 610, 755, 971, 4190 mK
Updated 1 May 2000, 16:55 PDT; corrected grp labels 25 June 2000

R = R0 exp(sqrt(T0/T))
G = G0 T^beta

                        R*     R
          R0    T0    0.3 K  0.5 K   G0=G(1 K)          G(0.3 K)*  G(0.5 K)
bol/grp  ohms    K    Mohms  Mohms  W/K^(beta+1)  beta     W/K       W/K
-------  ----  -----  -----  -----  ------------  ----  ---------  ---------
09 TH.4  1622  35.93   91.8   7.79     1.53e-9    1.67   0.20 e-9   0.48 e-9
10 TH.4  1658  35.50   87.9   7.57     1.52e-9    1.64   0.21 e-9   0.49 e-9
11 TH.4  1622  35.65   88.0   7.54     1.54e-9    1.69   0.20 e-9   0.48 e-9
12 TH.3  1800  34.29   79.1   7.11     1.42e-9    1.49   0.24 e-9   0.51 e-9
13 TH.3  1733  34.60   80.0   7.10     1.48e-9    1.53   0.23 e-9   0.51 e-9
14 TH.3  1726  34.57   79.3   7.05     1.49e-9    1.52   0.24 e-9   0.52 e-9
15 TH.3  1800  34.52   82.0   7.31     1.44e-9    1.51   0.23 e-9   0.51 e-9
16 TH.3  1802  34.41   80.7   7.22     1.44e-9    1.50   0.24 e-9   0.51 e-9
17 TH.2  1638  36.36   99.0   8.28     1.50e-9    1.57   0.23 e-9   0.51 e-9
18 TH.2  1668  36.19   98.2   8.26     1.49e-9    1.56   0.23 e-9   0.51 e-9
19 TH.2  1727  36.17  101     8.53     1.43e-9    1.56   0.22 e-9   0.48 e-9
20 TH.2  1693  36.09   98.2   8.29     1.46e-9    1.56   0.22 e-9   0.50 e-9
21 TH.2  1578  36.79  102     8.38     1.55e-9    1.62   0.22 e-9   0.50 e-9
22 TH.1  1096  33.11   40.0   3.75     1.42e-9    1.45   0.25 e-9   0.52 e-9
23 TH.1  1106  33.47   42.8   3.95     1.37e-9    1.42   0.25 e-9   0.51 e-9
24 TH.1  1108  33.03   40.0   3.75     1.37e-9    1.42   0.25 e-9   0.51 e-9

* extrapolation
Table 12. Four-parameter fits for thermistor test array 5347 RH7.

There is no strong resistance gradient across the RH7 thermistor device, as confirmed by the following 0.330 K measurements with an electrometer:

           Electrometer
            Resistance
Bolometer      Mohm
---------  ------------
    1          42.8
    6          44
   31          44
   32          35.0
Table 13. Electrometer resistance measurements for thermistor test array 5347 RH7.

Noise -- DC Bias

Noise for 5347 THUNIT2B.1
Figure 20. Noise spectra for bolometers 23-22 on 5347 thermistor test array RH7. The measurement technique and analysis are the same as in Figures 16 and 17. The bolometers are of type THUNIT2B.1 and have full-area thermistors. The predictions at right are for 10 Hz.

Noise for 5347 THUNIT2B.4
Figure 21. Noise spectra for bolometers 10-9 on 5347 thermistor test array RH7. The bolometers are of type THUNIT2B.4 and have small thermistors. The veritical display range has been enlarged by a factor of 2 compared to Figure 20.

Low Frequency Noise (AC Bias)

Differential AC-biased readout
Figure 22. Electronics configuration used to measure low-frequency noise. The amplifier circuit is the same as in Figure 16. Differences now are the AC bias on the detector and demodulation (in the DSP) prior to the Fourier transform (in software).

Noise for 5347 THUNIT2B.1 and .4
Figure 23. Low-frequency noise spectra for bolometers 23-22 and 10-9 on 5347 thermistor test array RH7. The noise has been divided by 21/2 and corrected for the amplifier gain to express the noise for a single bolometer. The predictions are based on the IV curves and the 1/f noise model of Han et al. (1998). For the bolometers with full-area thermistors, an NEP of 2x10-16 W s1/2 was observed at 0.01 Hz, and 9x10-17 W s1/2 at 0.1 Hz.

Time Constants

tau: bol. 23, 50 mV tau: bol. 10, 50 mV
Figure 24. Oscilloscope traces during time constant measurements of bolometers 23 (full area thermistor) and 10 (small thermistor) from thermistor test array 5347 RH7. The measurement technique was the same as in Figure 19. The bias frequency was 10 Hz. The transition times are similar.
                                                     calc.   observ.
            bias  calc G  calc T  V(o.s.)  t(o.s.)  V(step)  V(step)  t(settle)
bol.  grp.   mV    nw/K      K       mV      msec      mV       mV       msec
----  ----  ----  ------  ------  -------  -------  -------  -------  ---------
 10   TH.4   50*    0.34   0.40     1.3      1.3      0.82     0.80      3.6
 10   TH.4  100     0.47   0.49     1.1      0.36    -0.044   -0.025     2.1
 23   TH.1   50*    0.36   0.39     1.3      1.2      0.73     0.70      4.2
 23   TH.1  100     0.45   0.46     1.1      0.58     0.035    0.019     2.8

* optimum bias for NEP
Table 14. Time constant measurements for thermistor test array 5347 RH7 operated at 0.331 K.

At these temperatures, the size of the thermistor only plays a small role in the time constant and heat capacity -- 30% at most.


Results for 5347 thermistor test array RH7 with absorber

Thermistor array sample 5347 RH7 was returned to Goddard and coated on the back side with a 175 ohm (room temperature in air) Pd/Au film. The array was measured cold on June 22-23, 2000 in the same Caltech apparatus as above.

Similarity of Resistance and Thermal Conductance

The observed resistances before and after the absorbers were applied are essentially the same, indicating that radiation leaks onto the array are not a significant problem. The thermal conductances are also the same.
         before after  before after    before     after     before      after
           R*     R*     R      R
         0.3 K  0.3 K  0.5 K  0.5 K  G(0.3 K)*  G(0.3 K)*  G(0.5 K)   G(0.5 K)
bol/grp  Mohms  Mohms  Mohms  Mohms     W/K        W/K        W/K       W/K
-------  -----  -----  -----  -----  ---------  ---------  ---------  ---------
19 TH.2  101    115     8.53   8.59   0.22 e-9   0.18 e-9   0.48 e-9   0.49e-9
21 TH.2  102    117     8.38   8.47   0.22 e-9   0.18 e-9   0.50 e-9   0.51e-9
23 TH.1   42.8   46.9   3.95   4.07   0.25 e-9   0.21 e-9   0.51 e-9   0.48e-9
24 TH.1   40.0   43.5   3.75   3.94   0.25 e-9   0.21 e-9   0.51 e-9   0.49e-9
29 2B      NA    80.5    NA    6.44      NA      0.20 e-9      NA      0.55e-9
30 2B      NA    80.0    NA    6.55      NA      0.20 e-9      NA      0.53e-9
32 mem.    NA    68.5    NA    6.00      NA      9.12 e-9      NA     33.2 e-9

* extrapolation
Table 15. Comparison of resistance and thermal conductance measurements before and after application of Pd/Au absorbing film onto thermistor test array RH7.

Increased Time Constants

The time constants were 4-5 times higher, indicating a large heat capacity in the Pd/Au film.
                                   before      after
            bias  calc G  calc T  t(settle)  t(settle)
bol.  grp.   mV    nw/K      K       msec       msec  
----  ----  ----  ------  ------  ---------  ---------
 21   TH.2   76     0.44   0.46                  15
 23   TH.1   24     0.32   0.36                  16
 23   TH.1   50     0.36   0.39      4.2         19
 23   TH.1   76     0.42   0.43                  16
 23   TH.1  100     0.45   0.46      2.8         16
 30   2B     76     0.44   0.45                  15
Table 16. Comparison of time constants before and after application of absorbing film. The 'before' measurements had an operating temperature of 0.331 K, and the 'after' measurements had an operating temperature of 0.345 K.

tau: bol. 23, 75 mV
Figure 25. Oscilloscope trace during time constant measurements of bolometer 23 on thermistor array 5347 with an absorbing film. Compare with Figure 24, and note the change in horizontal scale (msec/division).


General Conclusions

The following conclusions apply to the operating temperatures of the measurements (0.33 - 1 K):
  1. Doping of ND = 0.75+-0.05 is suitable for HAWC and SHARCII. However, an accurate selection of doping is made difficult by the resistance variation across the 5347 (ND = 0.75) wafer.
  2. The 5327 (ND = 0.70) wafer had 0.3 K resistances of ~480 Mohms/square and 0.5 K resistances of ~22 Mohms/square.
  3. The 5347 (ND = 0.75) wafer had 0.3 K resistances of ~32 Mohms/square, but with a range of 9.7 to 70. The 0.5 K resistances were ~3.1 Mohms/square, with a range of 1.4 to 5.9.
  4. Bolometers with no metal on the torsion bars have thermal conductances with a T1.2 to T1.8 temperature dependence.
  5. Adding aluminum to the torsion bars significantly increases the thermal conductances and changes the temperature dependence to T2.0 to T3.6.
  6. Adding metal to the strap region has a minimal effect on the thermal conductance.
  7. The quantitative behavior of the thermal conductances is discussed below.
  8. The electrical time constants for the detectors at 0.4 K are approximately 1 msec for a G of 1 nW/K.
  9. The heat capacity from large thermistors is not significant compared to the rest of the pixel. The contribution of a full area thermistor is ~25% at 0.4 K.
  10. There is no evidence for excess noise in the bolometers in the white noise region (a few Hz to ~100 Hz). Electrical NEP's down to 6x10-17 W s1/2 have been observed.
  11. With a full-area thermistor, the useful bolometer signal band can be extended down to ~10 mHz, permitting scanning observing modes. The 1/f noise roughly follows the prediction of Han et al. (1998).

The most perplexing aspect of the detector measurements is the behavior of the thermal conductances, summarized in the table below:

                                tors. bar    tors. bar  G(0.3 K)*    G(0.5 K)
therm. struct.    wafer/sample  silicon W/L  metal W/L     nW/K         nW/K
----------------  ------------  -----------  ---------  ----------  -----------
HG2B, HG2C, TH2B  5327 G0 LH5      0.038       0        0.28- 0.38   0.66- 0.74
HG2B, HG2C, TH2B  5347 G0 LH1      0.038       0        0.22- 0.29   0.42- 0.53
HG2B, HG2C, TH2B  5347 th RH7      0.038       0        0.20- 0.25   0.48- 0.52

HG3C              5347 G0 LH1      0.068       0        0.51- 0.53   0.98- 1.02

HG3A              5347 G0 LH1      0.068       0.136^   0.69- 0.72   1.41- 1.50

HG1A              5327 G0 LH5      0.022       0.022    0.80- 1.02   3.91- 4.33
HG1A              5347 G0 LH1      0.022       0.022    0.71- 0.74   2.82- 2.99

HG2A, HG2D        5327 G0 LH5      0.038       0.038    1.53- 2.29   8.54-10.6
HG2A, HG2D        5347 G0 LH1      0.038       0.038    1.51- 1.62   5.85- 6.26

HG3B, HG3D        5347 G0 LH1      0.068       0.068    2.10- 2.30   5.69- 6.31

membrane          5327 G0 LH5      large       large    8.60-12.5   40.7 -52.4
membrane          5347 G0 LH1      large       large         10.9         24.4      

* extrapolation
^ only on cold half of torsion bar
Table 17. Summary of thermal properties of HGUNIT's and THUNIT's.

As noted in the section "Results for 5327 G0 Test Array LH5", the G's for metal-free legs go as ~T1.5, and the G's for the metallized legs go as ~T3. We have offered an explanation for the unexpected temperature dependence in that section.

The HGUNIT.2B/C, HGUNIT.3C, and HGUNIT.3A devices on 5347 G0 array LH1 can be used to estimate the dependence of G on torsion bar width and length for devices with no metal; we calculate a W1.06L-0.45 dependence at 0.3 K and W1.03L-0.53 at 0.5 K. (We have assumed that the metal half-way up the torsion bar on HGUNIT.3A is sufficient to cool that part of the bar to the base operating temperature.) In macroscopic/high temperature situations, we expect W1 and L-1, so the observed L dependence is surprising.

For the metallized devices (HGUNIT.1A, HGUNIT.2A/D, and HGUNIT.3B/D), the situation is even more surprising. The range of torsion bar lengths is not large, so we fit for the dependence of G on (W/L) together and calculate (W/L)0.99 at 0.3 K and (W/L)0.64 at 0.5 K, dominated presumably by width dependence. This is quite far from the expected (W/L)2 dependence. It is possible that the 0.5 K measurements of the metallized bolometers especially are contaminated by heating effects in the silicon frame and/or detector package.


Recommendation for SHARCII Bolometer Design

Following is the SHARCII bolometer design recommendation resulting from this study:

The following table summarizes the expected operating conditions of the SHARCII bolometers as designed above:

       parameter            value      units
-----------------------  ----------  ---------
operating temperature       0.32         K
T0                         40            K
R0                       1300           ohm
thermistor volume           2.7e-7      cm^3
G0                          1.9      W K^-2.35
beta (G = G0 T^beta)        1.35
R (load resistor)         200           Mohm
T (load resistor)           2.0          K
background power           75            pW
NEP (background)            4.4e-16   W s^1/2
voltage noise (amp.)        5  e-9    V s^1/2

V (bias)                  500            mV
V (bolometer)              19.4          mV
I                           2.4          nA
R (bolometer)               8.1         Mohm
Z (bolometer)               2.8         Mohm
T (bolometer)               0.52         K
G                           0.79        nW/K
S                           1.3e+8      V/W
NEP (detector, 0.01 Hz)     2.8e-16   W s^1/2
NEP (detector, 0.1 Hz)      1.4e-16   W s^1/2
NEP (detector, 1 Hz)        1.2e-16   W s^1/2
NEP (detector, 10 Hz)       1.2e-16   W s^1/2
det. volt. noise, 10 Hz    16  e-9    V s^1/2
time constant (elec.)       1           msec
Table 18. SHARCII bolometer characteristics, updated from Moseley et al. (1999).

Recommendation for HAWC Bolometer Design

TBD

References

Han, S.-I., et al. 1998, in EUV, X-Ray, and Gamma-Ray Instrumentation for Astronomy IX, ed. O. Siegmund & M. Gummin, Proc. SPIE 3445, "Intrinsic 1/f Noise in Doped Silicon Thermistors for Cryogenic Calorimeters"

Locatelli, M., Arnaud, D., & Routin, M. 1976, *journal unknown*, "Thermal conductivity of some insulating materials below 1K"

Mather, J. C. 1982, Applied Optics 21, 1125, "Bolometer noise: nonequilibrium theory"

Moseley, H. 1999, memo dated July 29, "Detector Design for HAWC"

Moseley, S. H, Dowell, C. D., Allen, C, & Phillips, T. G. 1999, in Imaging at Radio Through Submillimeter Wavelengths, ed. J. Mangum & S. Radford, ASP Conf. Ser., "Semiconducting Pop-Up Bolometers for Far-Infrared and Submillimeter Astronomy"

Toloukian, Y. S., Powell, R. W., Ho, C. Y., & Klemens, P. G. 1970, Thermal Properties of Matter, Volume 1, Thermal Conductivity -- Metallic Elements and Alloys, IFI/Plenum: New York

Wang, N., et al. 1996, Applied Optics, 35, 6629, "Characterization of a submillimeter high-angular-resolution camera with a monolithic silicon bolometer array for the Caltech Submillimeter Observatory"